Perhaps more importantly, it was Rothstein’s testimony that colorfully illustrated the extraordinary role that TD Bank played in Rothstein’s scheme. For example, after 1 h reaction at 100 °C with two equivalents of K2CO3, only unreacted aminosulfonamide was returned, and after 8 h a 40% conversion to the sulfinate salt was observed by 1H NMR spectroscopy. Fourier transform infrared spectroscopy implicated the role of carboxyl, amine and hydroxyl groups in the synthesis.
Chem. Rev. 110, 1147–1169 (2010). Zalesskiy, S. S. & Ananikov, V. P. Pd2(dba)3 as a precursor of soluble metal complexes and nanoparticles: determination of palladium active species for catalysis and synthesis. After 10 days, the orange needle-like crystals were formed. Curr. Chem. 1988, 144, 73–135. 7. Reissig, H.-U.; Zimmer, R. Chem. Sci., 2001, 57, 120 CrossRef CAS; (d) P. Boger, J. Pestic. Chem. 1984, 802–819. doi:10.1002/jlac.198419840416 Return to citation in text:  Khan, F. A.; Czerwonka, R.; Reissig, H.-U. Synlett 1996, 533–535. doi:10.1055/s-1996-5483 Return to citation in text:  Khan, F. A.; Czerwonka, R.; Reissig, H.-U. Eur. J. Org. The solution of AMMT (32.5 mg, 0.25 mM) in 15 ml of ethanol was slowly added to the hot reaction mixture under constant stirring.
Thus, UV-Vis data prove the similarity in structures of complexes in solid states and in solutions. Chem. Res. 2014, 47, 168–179. doi:10.1021/ar400104j Return to citation in text:   Zhao, Y.-B.; Mariampillai, B.; Candito, D. A.; Laleu, B.; Li, M.; Lautens, M. Angew. Below is a list of the nearly 30 individuals that have been arrested or convicted based on their connection to Rothstein: With some legal statutes of limitation expiring and prosecutors running out of individuals to charge, Rothstein’s role as government witness is likely nearing its twilight. Return to citation in text:  Yamamoto, Y.; Nakamura, I. Top.